Microstructure and Micromechanical Behaviors of Bulk Amorphous Alloy Prepared by Spark Plasma Sintering

Authors

  • Yaqiong Ge Taiyuan University of Science and Technology, College of Materials Science and Engineering, Taiyuan 030024, China
  • Zexin Chang Taiyuan University of Science and Technology, College of Materials Science and Engineering, Taiyuan 030024, China
  • Wenxian Wang Taiyuan University of Science and Technology, College of Materials Science and Engineering, Taiyuan 030024, China
  • Qingling Hou Taiyuan University of Science and Technology, College of Materials Science and Engineering, Taiyuan 030024, China

DOI:

https://doi.org/10.24425/amm.2023.141468

Abstract

This study aimed to prepare Zr55Cu30Al10Ni5 bulk amorphous alloys by spark plasma sintering of raw amorphous alloy powders and investigate their microstructure and micromechanical behaviors. When the sintering temperature ( Ts) was 675K, which was lower than the glass transition temperature ( Tg) of the material, the sintered sample was almost fully amorphous but the density was lower. However, when Ts was 705K, which was higher than Tg, partial crystallization occurred, but the density was higher. The hardness of the bonding zone of the sintered sample at 675K was 5.291 GPa due to the lower density, which was lower than that at 705K, and the hardness at 705K was 8.836 GPa. The generation of thermodynamically stable intermetallic phases, the hardness, and the elastic modulus of the samples sintered above Tg were higher due to the higher density.

Published

2023-03-06

How to Cite

Ge, Yaqiong, et al. “Microstructure and Micromechanical Behaviors of Bulk Amorphous Alloy Prepared by Spark Plasma Sintering”. Archives of Metallurgy and Materials, vol. 68, no. 1, Mar. 2023, doi:10.24425/amm.2023.141468.

Issue

Vol. 68 No. 1 (2023)

Section

Articles